Category: physical sciences retractions

Improper citation, PubPeer comment snowballs into double retraction in phys chem journal

chemphyschemChemPhysChem is retracting a pair of articles by a group of researchers in China and their colleagues who pieced together the work from two previously published articles.

The papers appeared in 2012 and 2015, and were flagged by a reader whose own work had been improperly cited, according to the editor of the journal.

The 2012 article was titled “Adsorption Features of Flavonoids on Macroporous Adsorption Resins Functionalized with Ionic Liquids,” and has been cited twice, according to Thomson Scientific’s Web of Knowledge. The senior author was Duolong Di, of the Lanzhou Institute of Chemical Physics in Qingdao. According to the retraction notice:
 Continue reading Improper citation, PubPeer comment snowballs into double retraction in phys chem journal

Third structure slip-up for chemist in Korea yields retraction

Chem_ak3Authors of a 2010 Chemistry – A European Journal article have retracted it “due to the wrong assignment of structure” of catalysts.

The retraction is the third, by our count, for corresponding author Doo Ok Jang, a chemist at Yonsei University in Wonju. Jang authored one of the previously retracted papers with Sung Jun Kim and the other with Sang Yoon Kim. Both papers were also sunk by misassigned structures.

The current study, “Enantioselective Radical Addition to Ketimines: A Synthetic Route Towards α,α-Disubstituted α-Amino Acids,” is authored by all three chemists. Here’s the retraction notice:

Continue reading Third structure slip-up for chemist in Korea yields retraction

Misconduct earns researcher a five-year ban on federal funding

ori logoA University of Minnesota former chemistry graduate student has been banned from receiving federal funding for five years based on “a preponderance of the evidence that the Respondent intentionally and knowingly engaged in research misconduct.”

Venkata J. Reddy appears to have manipulated findings in one R01 grant application. In recent years, bans are less common than having research supervised. What’s also unusual is that the sanction appeared to have begun two years ago, in 2013, because it lifts August 26, 2018. The report, which is scheduled to published tomorrow in the Federal Register, says the debarment has a “joint jurisdiction,” suggesting another agency may be involved. [See first update at end of post.]

According to the ORI notice, Reddy “intentionally and knowingly engaged in research misconduct by falsifying and/or fabricating data that was provided to his mentor” for an R01 application to the National Institute of General Medical Sciences (NIGMS). More specifically: Continue reading Misconduct earns researcher a five-year ban on federal funding

Chem paper fails to catalyze when wrong files are “inadvertently used”

joceah_v080i008.inddThree chemists at the Indian Institute of Technology Guwahati in India have retracted a paper from the Journal of Organic Chemistry because the “incorrect files were inadvertently used.”

The article, “Room-Temperature Cu(II)-Catalyzed Chemo- and Regioselective Ortho-Nitration of Arenes via C–H Functionalization,” described a protocol to perform nitration — the addition of nitro groups onto an organic compound — using an inexpensive copper catalyst.

All three authors signed the one-sentence notice:

Continue reading Chem paper fails to catalyze when wrong files are “inadvertently used”

Reporting errors sink chem paper on liquid-liquid equilibrium

Jced_coverA team of chemists at Hunan University and Zhejiang Shuyang Chemical Company in China have retracted a paper from the Journal of Chemical & Engineering Data after “inconsistencies with the literature” led them to discover “errors” in the way the data were reported.

According to the corresponding author Qinbo Wang, in December 2014, Robert Chirico, an associate editor at the journal, contacted Wang with concerns that the paper’s data were an anomaly.

Wang then went through the original notes with the first author, and realized that the data reported in the paper didn’t match the experimental results. The lab then conducted further experiments, and discovered that multiple corrections would be necessary. They were, as Wang told us: Continue reading Reporting errors sink chem paper on liquid-liquid equilibrium

Bielawski and Wiggins retraction count grows to six

chemical scienceA group of chemists whose work was investigated by the University of Texas-Austin has had another paper retracted, this one of a Chemical Science study previously subjected to an Expression of Concern.

That makes six retractions for Christopher Bielawski and Kelly Wiggins.

Here’s the notice for “Homonuclear bond activation using a stable N,N′-diamidocarbene”, signed by all three authors of the paper: Continue reading Bielawski and Wiggins retraction count grows to six

Controversial Italian scientist loses 11 papers from journal he used to edit

Alberto Carpinteri, via Politecnico di Torino
Alberto Carpinteri, via Politecnico di Torino

Alberto Carpinteri is something of a Renaissance man.

Along with championing a highly controversial form of energy generation called “piezonuclear fission,” which involves crushing rocks, the engineer has argued that the Shroud of Turin really is as old as Jesus, but carbon dating was thrown off by an earthquake.

Not everyone agrees with his ideas: In 2012, more than 1,000 scientists signed a petition asking the Italian National Institute of Metrological Research (or INRIM, of which Carpinteri was director at the time) not to fund piezonuclear fission.

Carpinteri was also editor in chief of the journal Meccanica until 2014, when Luigi Gambarotta took over. Now, Meccanica is retracting 11 of its former EIC’s papers, including the one on the Shroud, and a number on piezonuclear fission, which Wired Italy put on their list of “most famous science hoaxes.” The reason? According to the notice, “the editorial process had been compromised.” Continue reading Controversial Italian scientist loses 11 papers from journal he used to edit

Molecular mixup burns chemistry paper

advanced synthesis and catalysisChemists at Lanzhou University in China did the right thing last month, retracting a paper in Advanced Synthesis & Catalysis because of issues with a reactant that could only be corrected by changing “all the text and quantities.”

When the scientists were adding what was labeled Reactant 1 to the mix, they believed it was α-ethoxycarbonyl-α-azido-N-phenylacetamides. Unfortunately, what they were actually using was a decomposed version of the molecule, which threw everything off.

Here’s the notice for “tert-Butyl Hydroperoxide and Tetrabutylammonium Iodide- Promoted Free Radical Cyclization of α-Azido-N-arylamides”: Continue reading Molecular mixup burns chemistry paper

Retraction notice for steel manufacturing paper leaves much to the imagination

Screen Shot 2015-04-01 at 4.01.21 PMReading is hard and takes a long time, so it’s nice that the Iron and Steel Institute of Japan didn’t give us too much work to do with this 12 word retraction.

Journal ISIJ International minced no words about why the 2014 paper on steel manufacturing was withdrawn, because there were no words. Here’s the notice for “Microstructure and Properties of Fiber Laser Welded Joints of Ultrahigh-strength Steel 22MnB5 and its Dissimilar Combination with Q235 Steel” in its entirety – half the length of the title!: Continue reading Retraction notice for steel manufacturing paper leaves much to the imagination

Concurrent submission and publication squashes nano paper

CoverIssueJExptNanoSciA group of materials researchers at Solapur University in India have lost a paper because they submitted an identical manuscript to two journals. Both journals published the paper, though only one has retracted it.

Taylor and Francis journal Journal of Experimental Nanoscience retracted the 2012 paper in February this year; the notice doesn’t explain the delay, or how the editors learned about the overlap.

The retraction indicates the editor of the journal that published the other version of the paper was informed of the overlap, but the journal — – Journals of Materials Science: Materials in Electronics — has not issued a retraction.

Here’s the notice for “Development of nanostructured CdS sensor for H2S recognition: structural and physical characterizations”: Continue reading Concurrent submission and publication squashes nano paper