Category: ACS

Author who broke into lab to tamper with investigation now up to half a dozen retractions

Bioconjugate ChemistryKarel Bezouška, the scientist who tried to tamper with an investigation into his work by breaking into a lab refrigerator, has had his fifth and sixth papers retracted.

Here’s the notice from Bioconjugate Chemistry for 2012’s “Dimerization of an Immunoactivating Peptide Derived from Mycobacterial hsp65 Using N-Hydroxysuccinimide Based Bifunctional Reagents Is Critical for Its Antitumor Properties:” Continue reading Author who broke into lab to tamper with investigation now up to half a dozen retractions

Authors of “just make up an…analysis” Organometallics paper issue mega-correction

organometallicscoverBack in August we — and others — wrote about a paper in Organometallics for which one member of the study team appeared to have instructed a co-author to pad the article with artificial results. From the supplemental information (SI) of that paper:

Emma, please insert NMR data here! where are they? and for this compound, just make up an elemental analysis…

Now comes a correction statement from the group that can only be described as “mega.” First reported last month by Chemical & Engineering News, the lengthy notice begins: Continue reading Authors of “just make up an…analysis” Organometallics paper issue mega-correction

Karel Bezouška, who broke into lab to tamper with investigation, has JACS paper retracted

jacsat_v136i001.inddKarel Bezouška, who, as we noted last year “broke into a lab refrigerator so he could tamper with samples being used to try to replicate the experiments during the investigation,” has had his fourth paper retracted.

Here’s the notice, for “Synthesis of Multivalent Glycoconjugates Containing the Immunoactive LELTE Peptide: Effect of Glycosylation on Cellular Activation and Natural Killing by Human Peripheral Blood Mononuclear Cells,” in the Journal of the American Chemical Society (JACS): Continue reading Karel Bezouška, who broke into lab to tamper with investigation, has JACS paper retracted

Third retraction for Karel Bezouška, of lab break-in fame

bichaw_v052i049.inddWe’ve found a third retraction for Karel Bezouška, the Czech scientist, who, as we reported this summer, broke into a lab in an attempt to tamper with experiments trying to replicate his own falsified data.

The article, “Molecular Characterization of Binding of Calcium and Carbohydrates by an Early Activation Antigen of Lymphocytes CD69,” had appeared in 2003 in Biochemistry. and has been cited 29 times, according to Thomson Scientific’s Web of Knowledge.

Here’s the retraction notice: Continue reading Third retraction for Karel Bezouška, of lab break-in fame

Nano Letters retracts chopstick nanorod paper questioned this week on chemistry blogs

NANO LettersA chemistry paper on nanorods that became a lightning rod for criticism on chemistry blogs this week has been retracted.

Here’s the notice for “Chopstick Nanorods: Tuning the Angle between Pairs with High Yield,” originally published in June in Nano Letters by Rajasekhar Anumolu and Leonard F. Pease of the University of Utah: Continue reading Nano Letters retracts chopstick nanorod paper questioned this week on chemistry blogs

Carbon copies? Authors retract paper from leading chemistry journal

jacsat_v135i031.inddThe authors of a 2008 Journal of the American Chemical Society (JACS) paper have retracted it after a structure was “mistakenly assigned.”

The article, “Highly Enantioselective Radical Addition to N-Benzoyl Hydrazones Using Chiral Ammonium Salts,” was written by Doo Ok Jang and Sang Yoon Kim, chemists at Yonsei University, in Wonju. According to the abstract (which includes this molecular schema):

Continue reading Carbon copies? Authors retract paper from leading chemistry journal

Insert data here … Did researcher instruct co-author to make up results for chemistry paper?

orgnd7_v032i014.inddThe chemistry blogs have been buzzing this week with the story of a paper in the journal Organometallics that may — or may not — contain fabricated data.

But what makes the story a bit juicier — and yes, it’s sad that fabricated data is a bit ho-hum for us — is that one of the authors of the article appears to have been caught in the act of instructing the first author to make up results.

The article, “Synthesis, Structure, and Catalytic Studies of Palladium and Platinum Bis-Sulfoxide Complexes,” appeared last month and came from a group at the Institute for Organic Chemistry at the University of Zurich. The authors were Emma E. Drinkel, Linglin Wu, Anthony Linden and Reto Dorta.

As ChemBark reported earlier this week:

Continue reading Insert data here … Did researcher instruct co-author to make up results for chemistry paper?

Our bad! Researchers take colleagues’ data, lose paper

aamick_v005i012.inddA pair of chemists from China who published their colleagues’ data without knowledge or permission have lost the article to retraction. They also have another retraction on a similar topic, which we covered before.

The article, which appeared in ACS Applied Materials & Interfaces in 2012,  was titled “Nanoporous PtCo Surface Alloy Architecture with Enhanced Properties for Methanol Electrooxidation.” The authors, Huajun Qiu and Feixue Zou, are listed as being with the School of Chemistry and Chemical Engineering at Shandong University, in Jinan, China.

As the retraction notice states: Continue reading Our bad! Researchers take colleagues’ data, lose paper

Two retractions for scientist whose work is “not fully supported by the available laboratory records”

SK Manna
SK Manna

The head of immunology at India’s Centre for DNA Fingerprinting and Diagnostics, Sunil Kumar Manna, has retracted two papers for image problems.

Here’s the notice from Cell Death and Differentiation for “Inhibition of RelA phosphorylation sensitizes apoptosis in constitutive NF-kappaB-expressing and chemoresistant cells:” Continue reading Two retractions for scientist whose work is “not fully supported by the available laboratory records”

First author of recently retracted paper has another corrected, in J Ag Food Chem

jafcau_v061i004.inddA paper that shares a first author with a paper retracted in December has been corrected.

Late last year, we reported on a retraction in Antioxidants & Redox Signaling (ARDS) by Indika Edirisinghe, who was at the University of Rochester when the original paper was published, and colleagues. On January 17, the Journal of Agricultural and Food Chemistry published a correction to “Effect of Black Currant Anthocyanins on the Activation of Endothelial Nitric Oxide Synthase (eNOS) in Vitro in Human Endothelial Cells,” on which Edirisinghe is also first author.

His affiliation on that paper, originally published in July 2011, is the Illinois Institute of Technology. Here’s the correction: Continue reading First author of recently retracted paper has another corrected, in J Ag Food Chem